The objective of this study was to prepare, characterize and test the catalytic properties of iron and gallium salts of Aquivion® PFSA (hereinafter Aquivion-H). The samples were characterized by the determination of metal loading in fresh and used materials, ATR-FTIR, and thermogravimetric analysis (TG-DSC). The salts were screened in Friedel-Crafts acylation of some heterocyclic compounds and compared with some homogeneous and heterogeneous Lewis acids as well as with pure Aquivion-H. These new salts revealed efficient catalytic activity and recyclability.
Novel iron and gallium salts of Aquivion (R) PFSA: Synthesis, characterization and some catalytic applications
PICCOLO, Oreste;PAGANELLI, Stefano;BALLIANA, Eleonora;TASSINI, RICCARDO;RATHOD, VIKAS DAMU
2016-01-01
Abstract
The objective of this study was to prepare, characterize and test the catalytic properties of iron and gallium salts of Aquivion® PFSA (hereinafter Aquivion-H). The samples were characterized by the determination of metal loading in fresh and used materials, ATR-FTIR, and thermogravimetric analysis (TG-DSC). The salts were screened in Friedel-Crafts acylation of some heterocyclic compounds and compared with some homogeneous and heterogeneous Lewis acids as well as with pure Aquivion-H. These new salts revealed efficient catalytic activity and recyclability.
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